Abstract
AbstractUniformally 14C‐labelled 5‐hydroxymethyl‐2‐furaldehyde was synthesized by dehydration of D‐[U‐14C]fructose on an H+ ion exchange resin and a water isobutylmethyl ketone biphasic liquid reaction medium. The optimal reaction time was 45min, and after HPLC purification the radiochemical yield was 50%. The whole process took 2 hours.
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