Abstract
The Ni(II) Schiff base complex Ni(caph)(N3)(NO3), where caph = 2-amino-N-(3-phenylprop-2-enylidene)aniline, was synthesized and characterized by elemental analyses (CHN) and FT-IR spectroscopy. NiO nanoparticles were obtained by solid state thermal decomposition of Ni(caph)(N3)(NO3) at 450ºC. Their crystalline structures were characterized by X-ray diffraction (XRD), the morphology was characterized by scanning electron microscopy (SEM) and transmission electron microscopy (TEM), and the composition of the products was confirmed by FT-IR spectroscopy.
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