Abstract
A novel layered zinc phosphonate, Zn 2Cl[O 3PCH 2N(CH 2CH 2) 2O][O 3PCH 2NH(CH 2CH 2) 2O] 1 has been synthesized by hydrothermal reaction at 180 °C and structurally characterized by single crystal X-ray diffraction as well as with infrared spectroscopy, elemental analysis and thermogravimetric analysis. The interconnection of Zn(1)O 4, Zn(2)O 2NCl and CPO 3 tetrahedra via corner-sharing forms a double layer structure with a channel system along b-axis direction. The result of connections in this manner is the formation of 8- and 16-atom windows that are parallel to one another and run in the a-axis direction. The morpholinyl groups of the ligands are orientated toward the interlayer space.
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