Abstract
AbstractThe synthesis of controlled polystyrenes with different molecular weights has been performed in the presence of 1‐phenyl‐1‐(2,2,6,6‐tetramethyl‐1‐piperidinyloxy)ethane (PETEMPO). The polystyrenes have served as macroinitiators for the formation of poly(styrene‐b‐butyl methacrylate) block copolymers. Using differential scanning calorimetry (DSC) it has been shown that all block copolymers synthesized do not present phase segregation. © 2001 John Wiley & Sons, Inc. J Appl Polym Sci 82: 14–21, 2001
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