Abstract
Reaction of UCl4 with Li2fc·tmeda (fc = 1,1‘-ferrocenylene, tmeda = tetramethylethylenediamine) gave the tris(1,1‘-ferrocenylene) uranium complex [Li2(py)3U(fc)3] (1) (py = pyridine). X-ray analysis of a pyridine solvate of 1 revealed the propeller type structure of the U(fc)3 fragment, with the planar cyclopentadienyl rings of each fc group being parallel and with U−C and U−Fe bond distances of 2.52(7) and 3.14(2) A, respectively.
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