Abstract
Ammonium hexamolybdooxalatovanadate of the composition (NH4)3[V(C2O4)Mo6O18(OH)6] · 3H2O (I) has been synthesized and studied by mass spectroscopy, IR spectroscopy, thermogravimetry, and X_ray powder diffraction. Crystals of I are monoclinic with the unit cell parameters a = 11.9737 A, b = 18.6533 A, c = 11.2178 A, β = 121.021°, V = 3162. 95 A3, M = 1214.01 g/mol, ρcalcd = 1.91 g/cm3, and Z = 3.
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