Abstract
1. A practicable method for the synthesis of vicinal bis(difluoramino)-containing carboxylic acids by reacting tetrafluorohydrazine with unsaturated acids has been developed. 2. α,β-Bis(difluoramino)carboxylic acids are unstable and undergo decarboxylation followed by dehydrofluorination. 3. β,γ-Bis(difluoramino)carboxylic acids are fairly stable and in some cases display the properties of ordinary carboxylic acids.
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