Abstract
To determine the mechanism responsible for the formation of electrolytic sodium–vanadium oxide bronze e-Na x V2O5, synthesized earlier from acid vanadyl sulfate electrolyte, β-bronze i-Na x V2O5is synthesized by exposing electrolytic oxide e-V2O5in the same sodium-containing electrolyte under open-circuit conditions, with a subsequent annealing of the sample. It is established that the two modifications of β-bronze (e-Na x V2O5and i-Na x V2O5) are identical and that electrolytic precursors of β-bronze Na x V2O5form via an ion-exchange mechanism.
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