Abstract
The reaction of 3,4-thiophenedicarboxaldehyde and 1,3-diaminopropane in EtOH gives a tetraazamacrocylic ligand (L). Two NiII complexes of L were prepared by a simple addition reaction, while other macrocyclic NiII complexes were prepared by metal-controlled condensation reactions between 3,4-thiophenedicarboxaldehyde and aliphatic diamines. On the basis of various physical properties, the complexes can be described as six co-ordinate pseudo-octahedral structures. Simple reactions led to the isolation of isothiocyanate and percholorate derivatives.
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