Abstract
AbstractTritium‐labelled salmon calcitonin was synthesized successfully through a 5 step peptide synthesis. LC‐MS performed on each step played an important role for in process control. For accuracy, Q‐TOF MS was used to determine the specific activity of tritiated salmon calcitonin ([3H]SMC021) using the triple charged ion. Copyright © 2007 John Wiley & Sons, Ltd.
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