Abstract
Under polar conditions Cd(CF 3) 2 complexes react with (CO) 3CpMCl ( M = Mo, W) to form the corresponding M-CF 3 compounds. (CO) 3CpMoCF 3 is identified by comparing its spectroscopical data with the described ones. The 1H-, 13C, 13C, 19F-, and 183W-NMR spectra, the i.r. and mass spectra of the new compound (CO) 3CpWCF 3 are discussed. Both M-CF 3 compounds do not react as polar trifluoromethylation reagents.
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