Abstract

A compact snapshot of the current convergence of novel developments relevant to chemical engineering is given. Process intensification concepts are analysed through the lens of microfluidics and sonochemistry. Economical drivers and their influence on scientific activities are mentioned, including innovation opportunities towards deployment into society. We focus on the control of cavitation as a means to improve the energy efficiency of sonochemical reactors, as well as in the solids handling with ultrasound; both are considered the most difficult hurdles for its adoption in a practical and industrial sense. Particular examples for microfluidic clogging prevention, numbering-up and scaling-up strategies are given. To conclude, an outlook of possible new directions of this active and promising combination of technologies is hinted.

Highlights

  • Introduction and Definitions1.1 The Basics of UltrasoundWeber number (We) present in Fig. 1 a comprehensive diagram with terms and concepts that will be described and expanded in the text

  • We focus on the control of cavitation as a means to improve the energy efficiency of sonochemical reactors, as well as in the solids handling with ultrasound; both are considered the most difficult hurdles for its adoption in a practical and industrial sense

  • It will be clearer to the reader how synergy, understood in the framework of process intensification (PI), has the largest relevance when analysing the combination of microfluidics and ultrasound applications

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Summary

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Despite the wide use of cavitation, the borders between the physical and chemical phenomena remain blurred, which contributes to an extended use of sonochemistry in a black-box manner The reason behind this is that cavitation effects such as of liquid jets, streaming, chemical radical molecules production, plasma formation with light emission, and shockwaves, are intertwined in complex dependencies that are hard to resolve in space and time [13]. Users of sonochemistry and outsiders tend to confuse the definition of a bubble (gas in a liquid, or gas in gas as in soap bubbles) and cannot correlate a given effect with a specific phenomenon This situation has not prevented sonochemistry from being widely exploited in several useful applications, yet we think it could be done more efficiently

The Basics of Microreactors
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Synergistic Effects When Combining Ultrasound with Microreactors
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Economical Drivers and Scientific Impact
Integrating Ultrasound with Microfluidics
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Entangled Effects of Cavitation
Controlling Cavitation with Microscopic Crevices
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Batch Micro-Sono-Reactor
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Scaled-Up Non-Conventional Batch Reactor
Acoustic Streaming
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Clogging Prevention
Microfluidics As a Tool for Particle Synthesis
Outlook and Future Applications
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Introduction
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Findings
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Full Text
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