Abstract
The isolation of mono- and di- n-butylphosphoric acids from commercially available mixtures has been examined. A simple solvent extraction method based on the distribution of the acids between carbon tetrachloride-water, and diethylether-water, mixtures has been developed to obtain the individual acids with < 1 per cent of total (< 0·5 per cent acidic) impurities. A rapid paper chromatographic method of analysis is described which uses upward elution with a basic solvent mixture. The separated acids are then detected by spray reagents and the method allows approximately 0·5% v/v of each acid to be estimated visually in the presence of the other.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
