Abstract
Nanocrystalline α-NiS and β-NiS were synthesized through a solvothermal reducing process at 110 °C with ethanol and pyridine as solvent, respectively. X-ray diffraction (XRD), inductively coupled plasma-atomic emission spectra (ICP-AES) and transmission electron microscopy (TEM) were used to characterize the samples. In this reaction, due to the different properties of the solvents, solvent determines the phases of as-prepared NiS. And it was found that the as-prepared α-NiS had higher phase stability than the normal NiS.
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