Abstract
A β-phase of sodium-vanadium oxide bronze thin film has been synthesized by using sol–gel technology from V2O5 and Na2SO4. The powders of these materials in suitable proportion were dissolved in hydrogen peroxide and heated up to 350 K for the dissociation of peroxide complexes. The obtained gel was deposited onto a metallic substrate and dried in air at room temperature. The produced xerogel was heated up to 580 K in air atmosphere for the removal of water from xerogel. Starting materials, xerogel, as well as a final product were investigated by means of X-ray photoelectron spectroscopy method. X-ray photoelectron spectra testify that the chemical bonds of vanadium, oxygen and sodium in the bronze differ from the similar bonds in the starting materials. The sulphur presence was detected in the xerogel but not in the final bronze composition.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.