Abstract
Dynamic information can be obtained on in-progress reactions in real time using a balloon-pressurized Schlenk flask in combination with an electrospray ionization mass spectrometer. The apparatus can be set up on a Schlenk line or in a glovebox and transported to the spectrometer, to be initiated by addition of catalyst or reactant by syringe through a septum. The system is demonstrated on palladium-catalyzed oxidation of phosphines.
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