Abstract

NiO with spherical-like morphology were prepared by microwave irradiation using Ni(II) acetate, water as solvent and sodium hydroxide (NaOH) as precipitator agent. Structural, optical and nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), UV–Vis absorption; Fourier transformed infrared (FTIR). The XRD pattern studies revealed the NiO have a face-centered cubic structure. The composition of nanostructures confirmed by analysis of FTIR spectra. The average size of the NiO nanoparticle observed from SEM images is found to be dimensions about 20 nm.

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