Abstract
A first attempt at the separation of fructo-oligosaccharides (FOS) and inulin mixtures is presented. Preliminary results obtained by automated multiple development (AMD) of diol layers with an acetonitrile-acetone-water polarity gradient are reported. The method is very promising and highly suitable for simple, direct analysis of complex mixtures of fructo-oligosaccharides (FOS) and inulin in samples of natural origin.
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