Abstract
AbstractWe describe a selective method for synthesis of 4‐chalcogenylmethyl‐1,3‐dioxolan‐2‐ones and 1,3‐bis(organylchalcogenyl)propan‐2‐ols in a short reaction time through stoichiometric control. The use of 3‐O‐tosyl glycerol 1,2‐carbonate and a set of aryl and alkyl diorganyl dichalcogenides afforded the desired products in good to excellent yields. We also describe a synthetic application to 4‐chalcogenylmethyl‐1,3‐dioxolan‐2‐ones by base promoted the synthesis of 3‐(arylchalcogenyl)propane‐1,2‐diols in excellent yields.
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