Abstract
The transformation of yellow goethite into red hematite by heating has long been assumed for Palaeolithic red artefacts excavated close to fireplaces. However, this transformation is extremely rare. Using SEM–FEG–EDX, PIXE–PIGE, TEM and μXRD, we characterized the mineralogical and chemical compositions of four microsamples of colouring materials from the Mousterian layer B in the es‐Skhul rock‐shelter, from about 100 kya ago. For some colouring materials, the Mousterian people of es‐Skhul chose to gather remote yellow lumps for heating. Their significant transport distance provides evidence of the possible high cultural value of these colouring materials for transformation into red pigments.
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