Abstract
Measurements of X-ray diffraction (XD) on 1 and 3 M Sc(CIO 4) 3 aqueous solutions and of X-ray absorption fine structure (XAFS) on a 4.6 M Sc(CF 3SO 3) 3 aqueous solution have been made at room temperature. Both the XD and XAFS data have revealed that about seven water molecules are bound to a Sc 3+ ion with a Sc 3+−H 2O distance of 2.18 Å. The results are discussed with those obtained by Raman spectroscopy and single crystal X-ray diffraction.
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