Abstract
Reductive N-alkylation of the ‘amide’ anchor resin, 9-amino-xanthen-3-yloxymethyl poly(styrene)1, by sequential treatment with alkyl aldehydes under mild acidic conditions followed by NaBH4 in MeOH–DMF, and then followed by optimised Fmoc/But solid-phase peptide synthetic procedures afforded an unique class of peptidyl N-alkyl amides in excellent yields.
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