Abstract
C 13 H 9 N, M r =179.22, orthorhombic, P2 1 2 1 2 1 , a=4.872 (2), b=11.526 (4), c= 15.811 (4) A, V=887.7 (5) A 3 , Z=4, D x = 1.341 Mg m -3 , λ(Mo Kα)=0.71069 A, μ= 0.07 mm -1 , F(000)=376, T=110 K, final R=0.045 for 1713 observed reflections. Phenanthridine was found to be planar in the solid state with a mean deviation of 0.002 A from the mean plane of the C and N atoms. The geometries of the benzene fragment in the molecule are rather similar and in the central pyridine moiety the C-N bond lengths are typical of C-N single and double bonds
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