Abstract
Chlorine monofluoride reacts with tetrasulphur tetranitride to give thiazyl chloride (monomer and trimer) and thiazyl fluoride; with further ClF, NSCl reacts to form NSF then ClNSF 2, and finally N 2, Cl 2 and SF 4. The reaction NSCl/ClF to give NSF/Cl 2 reverses in SO 2 solvent due to removal of ClF as SO 2ClF. NSF was prepared, in a new method, by passing NSCl through a column of CsF at 110°.
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