Abstract
The compound (onH 2)[Ni 2Cl 6 (H 20) 2] ( I), where on = 1,8-octamethylenediamine, is obtained as flat yellow crystals by reaction between nickel(II) chloride hexahydrate and the hydrochloride of the diamine. Dehydration of compound I leads to the reddish-yellow anhydrous compound (onH 2)[NiCl 3]2 ( II). Both compounds show diffuse reflectance spectra and magnetic moments typical of nickel(II) in an octahedral environment. The compounds were also studied by IR spectroscopy, differential thermal analysis and thermogravimetric analysis.
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