Abstract

Fine-grained micro-potassium doped tungsten samples were sintered by spark-plasma-sintering (SPS) method using tungsten–potassium (W–K) mixed powder. The potassium content, microstructure, density and mechanical properties of the sintered samples were measured. It is found that both sintering temperature and pressure play important roles to obtain high-density and fine-grain sample. By one step sintering method, the relative density (95.6%) and Vickers hardness (350.8) of the sample are largely improved than those of the commercial W–K (91.74% and 291.9, respectively) at similar grain size. Through two-step sintering, its grain size becomes smaller and more homogenous than that of the commercial one while showing similar density. This study will provide a novel way to fabricate high-density/fine-grain plasma facing material W–K.

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