Abstract
The separation of Tc(VII) from Mo(VI) by thin-layer and paper-chromatography is discussed. Some aspects concerning the formation and identification of lower oxidation states of Tc(VII) are also mentioned. Finally, a spot test is recommended for the determination of Mo(VI) and Al, which can be contaminants in the Tc(VII) solution eluted from the99Mo column, filled with Al2O3.
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