Abstract
X-ray and EXAFS data reveal that the metal skeleton in the palladium carbonyl acetate cluster, Pd 4(CO) 4(OAc) 4, undergoes significant changes upon replacement of the CO and AcO groups. The rectangular skeleton rearranges into a square one when Pd 4(CO) 4(OAC) 4 is stored at room temperature, showing non-rigity of the cluster core and the ability of the ligands to migrate.
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