Abstract
• A general and straightforward palladium-catalyzed aminocarbonylation procedure of benzyl chlorides have been developed. • o- nitrobenzaldehydes have been used as stable nitrogen sources for the synthesis of 3-arylquinolin-2(1 H )-ones. • Mo(CO) 6 has been used both as CO precursor and reductant. A palladium-catalyzed carbonylative cyclization of benzyl chlorides with o- nitrobenzaldehydes has been developed for the synthesis of 3-arylquinolin-2(1 H )-ones. Mo(CO) 6 played a dual role as both a CO surrogate and a reductant in this carbonylative transformation.
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