Abstract
Mössbauer spectroscopy in external magnetic fields has been used to measure the signs of the principal components of the electric field gradient V zz in the two forms of [Fe(H 2O) 6)(C10 4) 2. The signs are V zz negative for the (B) with Δ E B = 1.4 mm/sec. This implies a trigonally distorted ligand field and the transition (A) → (B) corresponds to compression → elongation with respect to the trigonal axis.
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