Abstract
Various substituted benzo-mono-, bis-, and tris-1,2,3-trithioles were synthesized by reaction of the corresponding thiolates with sulfur dichloride. Benzo-bis(trithiolo)pentathiepin was isolated as a by-product. These trithioles form with cyanide dibenzo[c,g]1,2,5,6-tetrathiocines and afforded with antimony pentachloride stable radical cations. Some EPR and conductivity data are reported.
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