Non-contact characterisation of conductivity gradient in isotropic polycrystalline graphite using inductance spectroscopy measurements

Abstract

The two main graphite ageing processes in advanced gas-cooled reactors (AGRs) are fast neutron damage and radiolytic graphite oxidation. These processes change the properties of the graphite core and lead to a reduction in the graphite density, ie a weight loss. Electrical conductivity measurement of the graphite material is among the possible methods for estimating the weight loss and hence provides a measure of the graphite ageing. The inductance spectroscopy technique using eddy current sensors has been implemented in a wide variety of NDT applications, since it enables the possibility of extracting the electrical parameters variation from eddy current measurements and examining more fully the internal material structure. In this paper we present a non-contact eddy current method for determining non-destructively the electrical conductivity gradient through 100 mm-thick graphite sections using inductive spectroscopic measurements collected by a gradiometer. The method employs the commercial finite element software COMSOL to generate the data from a model of a real profile distribution. This data is translated to the profile conductivity of the graphite test object via the solution of an inverse problem. The linear Tikhonov regularisation method and the non-linear regularised Gauss Newton technique are employed in the solution of the inverse problem. During the optimisation, the forward problem is evaluated using COMSOL. Numerical optimisation tests have been carried out for different cases of step conductivity profiles. Initial results using simulated data show that representative estimates of the conductivity profile of the modelled graphite sections have been obtained.