Abstract
(NH4)3FeF6 mesocrystalline octahedrons are formed by in situ dissolution and the reaction of anodic iron oxides, followed by a non-classical crystal growth process involving electrical polarization and subsequent alignment of primary (NH4)3FeF6 particles under an external electric field. The obtained (NH4)3FeF6 can be converted to nano-micro hierarchical α-Fe2O3 octahedrons by thermal annealing.
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