Abstract
Cyclic ether formation by dehydration of a cis-fused 5-acetyl-1,5-dihydroxyoctahydronaphthalene occurs with rearrangement to give a 12-oxatricyclo[5.4.1 1,7.O 3,8]dodecene rather than the 11-oxatricyclo[4.4.1 1,6.O 2,7]undecene system of the nargenicin antibiotics.
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