Abstract
The infrared spectra of the monohydrates of sodium and potassium thiosaccharinates and of some of their partially deuterated analogues were recorded at room and liquid-nitrogen temperatures. The spectral features in the OH and OD stretching regions were correlated with the crystallographic data on the geometry of the water molecules and their nearest neighbours. In an attempt to assign the bands due to the SO 2 stretching modes, the spectra of the thiosaccharinates were compared with those of the hydrate of sodium saccharinate, Na 3(C 7H 4NO 3S) 3 · 2H 2O.
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