Abstract

In a unique temperature dependent reversible reaction, the bicyclo[2.2.2]organoiron complex 8 is assembled from three molecular components, i.e. the Fe(CNR)3(α-diimine) complex 1b, dimethyl maleate and 2,6-xylyl isocyanide, and disassembled again via consecutive organometal 1,3-dipolar concerted cycloaddition–reversion and isocyanide insertion–deinsertion reactions.

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