Abstract

Mesoporous V-MCM-41 materials with good hydrothermal stability had been synthesized by microwave-assisted hydrothermal method. The samples by microwave-assisted hydrothermal synthesis and conventional heating remain the same mesoporous structure by XRD and N2adsorption analysis. The V-MCM-41 materials by microwave-assisted hydrothermal synthesis show the good hydrothermal stability, close to that of the materials by conventional heating. The high surface area of the sample by 720 W microwave treatment for 8 min was the same as that of the sample by conventional heating (110 °C for 12 h).

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