Abstract
In order to better understand the micropore structure of shale reservoir in Jiyang Depression, permeability damage test, low temperature nitrogen adsorption and scanning electron microscopy (SEM) were carried out on six cores in the target block. The adsorption isotherms were analyzed by Frenkel–Halsey–Hill (FHH) model, and the fractal dimensions of different layers were calculated. The results show that the shale pore system is mainly composed of organic nanopores, inorganic nanopores and micro-fractures. The inorganic pores are mainly distributed around or inside the mineral particles, while microcracks are commonly found between mineral particles or at the organic–mineral interface. Organic pores are located within or between organic particles. The results of nitrogen adsorption show that the shale pores are mainly H2/H3 hysteresis loops with wedge, plate or ink bottle shapes. The pore structure is highly complex, and the fractal dimension is high. The mean D1 fractal dimension, which represents pore surface roughness, is 2.3788, and the mean D2 fractal dimension, which represents pore structure complexity, is 2.7189. The fractal dimension is positively correlated with specific surface area and total pore volume and negatively correlated with average pore radius. The permeability damage rates of the N layer, B layer, and F layer are 17.39%, 20.2%, and 21.6%, respectively. The contact Angle of the core decreases with the increase in water skiing time. In this study, the micropore structure of different formations in Jiyang Depression is compared and analyzed, which provides valuable insights for the optimization and differentiated development of shale oil and gas resources.
Published Version
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