Abstract
An automatic reaction-rate method is described for the microdetermination of molybdenum; the method is based on the hydrogen peroxide-iodide reaction which is catalyzed by molybdenum. The effect of reagent concentrations was studied and the maximum tolerable amounts of interfering ions were determined. Procedures for the determination of 0.01–0.15 μg and 0.1–1.0 μg molybdenum per milliliter are given ; 0.036–2.5 μg of molybdenum could be determined with relative errors of about 2%.
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