Abstract
Solid Phase Extraction is a method used for extraction, purification of compounds contained in complex matrices and purification of samples in the fields of industry, pharmacy, and toxicology analysis. This review represents the recent advances of solid phase extraction from different mode of separation which are the most commonly used in recent days such as molecular imprinting solid phase extraction (MISPE), magnetic solid phase extraction (MSPE) and matrix solid phase dispersion (MSPD). In this review, the applications of MISPE in the analysis of agrochemicals such as herbicides, fungicides and insecticides are summarized. This review also states preparation of various magnetic composites (MSPE) based on graphene and its application as adsorbents in pre concentrating natural mixes, organic macromolecules. Besides this, this review summarizes the application of MSPD in biological, food, and environmental samples, including both organic and inorganic analyte.
Highlights
A method utilized for extraction, sanitization of compounds contained in complex matrices and purification of samples in the fields of industry, pharmacy, and toxicology analysis is called strong stage extraction
Our review is based on the literature obtained from the PubMed and Scopus databases using the keywords “molecular imprinted solid phase extraction”, “matrix solid phase dispersion” and “magnetic solid phase extraction”
The specific keywords related to application of molecular imprinted solid phase extraction, matrix solid phase dispersion and magnetic solid phase extraction used were “molecular imprinted solid phase extraction in complex matrices,” “magnetic solid phase dispersion in food,” “molecular imprinted solid phase extraction in biological fluid,” and “matrix solid phase dispersion in pharmaceuticals
Summary
A method utilized for extraction, sanitization of compounds contained in complex matrices and purification of samples in the fields of industry, pharmacy, and toxicology analysis is called strong stage extraction. It is the most generally utilized analytical extraction strategies and can facilitate the analysis of a compound from biological materials such as blood, urine, water, etc. SPE has the advantage when compared to liquid-liquid extraction that is by using SPE the extraction process becomes more perfect, the separation of analyte from the matrix becomes more efficient, reducing the organic solvents used. The advantages when compared to other methods such as HPLC, NMR, and MS are low costs, the ability and sample analysis are quite good [2]
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