Abstract
In this chapter we present an overview over different designs and approaches to couple electrochemical measurements and mass spectrometry for the online monitoring of reaction product and intermediate formation. We cover the method development from the early attempts to the most recent and advanced applications, where hyphenation with additional analytical and spectroscopic techniques allows for detailed kinetic and mechanistic studies of complex processes occurring at the electrochemical interfaces. Applications mainly include studies of electrocatalytic reactions and electrochemical conversion reactions relevant for energy conversion and energy storage devices. We will discuss the related challenges, both in aqueous and organic or solid electrolytes, respectively, as well as the trends for further developments.
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