Abstract
Flow pyrolysis of some 2-aryloxy-1,3,2-dioxaphospholanes with ortho-CF 3 or F substituents, either alone or in the presence of methanol, has provided evidence for the formation of metaphosphates as intermediates; these highly reactive species then undergo further reaction, depending on the nature of the substituent. Mass spectrometric studies of the starting materials have also suggested the elimination of ethylene and the formation of metaphosphates to a limited extent.
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