Abstract

Ni-based industrial alloy samples (INCONEL® 601) were subjected to oxidizing conditions, followed by exposure to a high carbon activity gaseous mixture containing 10% CO in Ar at 550°C in order to reveal factors critical to the initial carbon-formation. Fresh and treated samples were studied via optical-microscopy, SEM, Auger depth-profile analysis, TEM and EPMA. The results show that the extent of carbon formation is dependent on the oxidation parameters, since these affect both the composition and the structure of the 20-60nm thick oxide layer formed. A high oxygen partial pressure during oxidation appears to promote inclusion of Ni or Fe species in the oxide, which subsequently reduce and catalyse the growth of carbon filaments. Surface pre-treatment (i.e. polishing before oxidation) is also found to affect the carbon formation.

Full Text
Paper version not known

Talk to us

Join us for a 30 min session where you can share your feedback and ask us any queries you have

Schedule a call

Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.