Abstract
A two-photon lonization technique has been developed and applied to determine the photoionization threshold of a molecule in liquid solution. The photoionization of pyrene in n-pentane was studied by monitoring the photocurrent of an≈ 10 −6 M solution as a function of the laser wavelength in the region 360–530 nm, corresponding to two-photon, transition in the region 180–265 nm. The photoionization threshold thus determined is 4.80 ± 0.02 eV. Resonances were observed in the two-photon ionization spectrum which are tentatively ascribed to preionization of one-photon forbidden transitions to states energetically degenerate with the continuum, reached via two-photon absorption.
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