Abstract
Irradiation induced structural changes in multilayered W/ZrO2 nanocomposites with periodic bilayer thicknesses of (7/14nm) and (70/140nm) were investigated following Au+ ion irradiation. The samples were irradiated by 4MeV Au ions with fluences ranging from 6×1014 to 1×1016ions/cm2. The immiscible W/ZrO2 interfaces remained unchanged without intermixing of the layers upon the irradiation. No voids were observed in the samples with different periodic layer thicknesses. The XRD and XTEM studies reveal thickness dependent microstructural changes in the samples. W and ZrO2 grains in the thinner (7/14nm) bilayer sample exhibit significant resistance to grain growth compared to the thicker (70/140nm) bilayer sample as well as a W monolayer film. The high fraction of flat interfaces as well as grain boundaries in multilayer films plays a role in suppressing ion irradiation-induced grain growth and void formation.
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