Abstract
The synchrotron x-ray source provides a unique opportunity to observe many “in-situ” processes. The formation of the “short-lived” intermediate species, Ta2C, during the combustion synthesis of TaC, has been observed and reported by monitoring the Bragg diffraction peaks of the reactants and products, Similarly, the synthesis of the ferroelectric material, BaTiO3, and subsequent phase transfonnation from cubic to tetragonal have also been investigated. These experiments would not have been possible without the high incident x-ray flux available at a synchrotron source.
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