Abstract
We have investigated the formation and reactivity of new metastable phases using mild hydrothermal synthesis. Following the characterization of two new open structure sodium tungsten oxides, we found that by using a small cationic template we were able to synthesize a new layered structure titanium phosphate. Preliminary chemical analysis of this compound indicates that its hydrogen form has the formula TiO(OH)(H 2PO 4)·2H 2O. 31P MAS-NMR indicates that each phosphorus has two OH groups. This sold acid is readily swelled on reaction with organic amines.
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