Abstract
CsNiP and 2(LiZnHP2O7) crystals were synthesized by hydrothermal technique at moderate P-T conditions. Solubility results of both the compound shown positive thermal coefficient and single crystal X-ray studies revealed, CsNiP crystallized in hexagonal system with cell parameters; a = 7.173(2), c = 5.944(9) A, V = 264.87(7) A3 and space group P63/mmc and 2(LiZnHP2O7) crystallized in orthorhombic system with cell parameters; a = 12.3636 A, b = 27.5330 A, c = 6.8647 A and space group, Pca21 exhibiting ring type of cavities with open aperture in the structure. CsNiP is a frequency dependent paramagnetic and 2(LiZnHP2O7) is a diamagnetic.
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