Abstract
GL-MS spectroscopy and conductivity measurements were used to study solutions of aluminum bromide in benzene, toluene, xylene, and methyl iodide. It was shown that AlBr3is transformed most considerably in xylene solutions. Aluminum began to precipitate from xylene-based electrolytes immediately after their preparation. The current efficiency increased from 40 to 80% with the electrolysis time. The resulting solutions contained about 20 compounds. Aluminum precipitation is accompanied by transalkylation, alkylation, bromination, and polymerization, suggesting the electrolytic mechanism of aluminum plating.
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