Abstract
Another new Ru 2 (xhp) 4 type compound, Ru 2 (fhp) 4 (thf) (fhp − =6-fluoro-2-hydroxypyridinate), has been prepared from Ru 2 -(O 2 CCH 3 ) 4 and characterized by X-ray crystallography and magnetic susceptibility measurements from ca. 5 to ca. 300 K. Dark brown Ru 2 (fhp) 4 (thf) crystallizes in space group P2 1 2 1 2 1 with a=16.392 (4) A, b=17.161 (5) A, c=9.148 (2) A, V=2573 (1) A 3 , and Z=4. The structure determined has Ru-Ru=2.274 (1) A and a polar ligand arrangement placing all like atoms (i.e., N's or O's) on the same metal centers
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